Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SEALED TUBE |
| Source details | OXFORD DIFFRACTION ENHANCE ULTRA |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2017-07-12 |
| Detector | OXFORD ONYX CCD |
| Wavelength(s) | 1.540 |
| Spacegroup name | P 1 |
| Unit cell lengths | 38.111, 43.048, 59.281 |
| Unit cell angles | 77.92, 75.63, 71.67 |
Refinement procedure
| Resolution | 56.840 - 2.300 |
| R-factor | 0.208 |
| Rwork | 0.206 |
| R-free | 0.22800 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.070 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXD |
| Refinement software | BUSTER (2.10.3) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 56.840 | 2.360 |
| High resolution limit [Å] | 2.300 | 2.300 |
| Rmerge | 0.190 | 0.880 |
| Number of reflections | 14998 | |
| <I/σ(I)> | 6.5 | 1.2 |
| Completeness [%] | 98.5 | 97.5 |
| Redundancy | 11.9 | 11.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 293 | 0.1 M HEPES, 20% PEG 6000, PH 7.0, VAPOR DIFFUSION, SITTING DROP, TEMPERATURE 293K |
