Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-09-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.972420 |
| Spacegroup name | P 1 |
| Unit cell lengths | 37.280, 43.250, 55.300 |
| Unit cell angles | 94.88, 93.25, 108.18 |
Refinement procedure
| Resolution | 40.849 - 1.750 |
| R-factor | 0.1758 |
| Rwork | 0.175 |
| R-free | 0.19710 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 5OLI |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.145 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | PHENIX ((dev_3366: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.850 |
| High resolution limit [Å] | 1.750 | 1.750 |
| Rmerge | 0.070 | 0.650 |
| Number of reflections | 31785 | 4346 |
| <I/σ(I)> | 15.7 | 2.6 |
| Completeness [%] | 96.7 | 95.6 |
| Redundancy | 4.5 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 293 | 0.1 M MES, 20% PEG3350 |
