6Q3V

Crystal structure of Human N4BP1 KH domains

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	BESSY BEAMLINE 14.1
Synchrotron site	BESSY
Beamline	14.1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-12-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.91841
Spacegroup name	P 62
Unit cell lengths	108.690, 108.690, 27.727
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	35.577 - 1.882
R-factor	0.1831
Rwork	0.181
R-free	0.23100
Structure solution method	SAD
RMSD bond length	0.006
RMSD bond angle	0.951
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.060	1.950
High resolution limit [Å]	1.882	1.882
Rmeas	0.063
Number of reflections	15568
<I/σ(I)>	19.78
Completeness [%]	99.7
Redundancy	6.51

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	Sodium malonate