6Q37
Complex of Arginase 2 with Example 23
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-20 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.54178 |
Spacegroup name | P 42 21 2 |
Unit cell lengths | 128.162, 128.162, 158.985 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 26.496 - 2.211 |
R-factor | 0.1503 |
Rwork | 0.148 |
R-free | 0.18940 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1d3v |
RMSD bond length | 0.008 |
RMSD bond angle | 1.068 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.079 | 0.285 |
Total number of observations | 747806 | |
Number of reflections | 63343 | 7066 |
<I/σ(I)> | 30.7 | 7.9 |
Completeness [%] | 93.8 | 60.5 |
Redundancy | 11.8 | 10.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | CRYSTALS IN CONDITION H3 FROM SILVER BULLET SCREEN (HAMPTON RESEARCH) USING TACSIMATE |