6PRO

MnSOD from Geobacillus stearothermophilus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SEALED TUBE
Source details	OTHER
Temperature [K]	293
Detector technology	DIFFRACTOMETER
Collection date	1981-02-02
Detector	hilger and watts
Wavelength(s)	1.5406
Spacegroup name	P 21 21 2
Unit cell lengths	72.200, 111.100, 51.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.049 - 2.263
R-factor	0.1559
Rwork	0.154
R-free	0.19610
Structure solution method	MIR
Data reduction software	MOSFLM
Data scaling software	in-house
Phasing software	in-house
Refinement software	PHENIX (1.14_3247)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.050	2.870
High resolution limit [Å]	2.260	2.260
Rmerge	0.068
Number of reflections	16562	6730
<I/σ(I)>	8.3
Completeness [%]	83.5	67.8
Redundancy	5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	BATCH MODE		293	25-30% PEG6000, 50 mM imidazole