6ORJ

Central spike of phiKZ phage tail

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	CCD
Collection date	2011-10-22
Detector	MARMOSAIC 225 mm CCD
Wavelength(s)	0.97920
Spacegroup name	P 63 2 2
Unit cell lengths	82.595, 82.595, 345.930
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.889 - 2.370
R-factor	0.1768
Rwork	0.175
R-free	0.20580
Structure solution method	SAD
Data reduction software	XDS
Data scaling software	XDS
Phasing software	SHELXDE
Refinement software	PHENIX (1.14-3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.510
High resolution limit [Å]	2.370	2.370
Rmerge	0.082	0.876
Rmeas	0.086	0.890
Number of reflections	51342	6654
<I/σ(I)>	22.92	1.85
Completeness [%]	95.1	76.1
Redundancy	10.1	5.65

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	293	4 M sodium chloride, 100 mM CHES, pH 9.0, 0.3% w/v sorbitol or adonitol