6OIZ

Amyloid-Beta (20-34) wild type

Experimental procedure

Source type	ELECTRON MICROSCOPE
Source details	FEI TALOS ARCTICA
Detector technology	CMOS DETECTOR
Collection date	2019-03-21
Detector	FEI CETA (4k x 4k)
Wavelength(s)	0.0251
Spacegroup name	P 1 21 1
Unit cell lengths	33.170, 4.780, 30.330
Unit cell angles	90.00, 111.10, 90.00

Refinement procedure

Resolution	7.737 - 1.100
R-factor	0.1963
Rwork	0.194
R-free	0.21260
Structure solution method	AB INITIO PHASING
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	SHELXD
Refinement software	PHENIX (dev_3360)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	7.737	7.737	1.130
High resolution limit [Å]	1.100	4.920	1.100
Rmerge	0.189	0.133	0.459
Rmeas	0.204	0.155	0.498
Total number of observations	23638
Number of reflections	3546	26	255
<I/σ(I)>	5.41	6.87	3.28
Completeness [%]	85.2	42.6	81.7
Redundancy	6.666	3.385	6.141
CC(1/2)	0.987	0.982	0.828

Crystallization Conditions

crystal ID	method	pH	temperature	details
1