6OBS
PP1 Y134K
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | LIQUID ANODE |
| Source details | BRUKER METALJET |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-05-31 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.34 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 65.094, 76.794, 131.567 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 17.730 - 1.803 |
| R-factor | 0.2064 |
| Rwork | 0.204 |
| R-free | 0.24610 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4mov |
| RMSD bond length | 0.010 |
| RMSD bond angle | 0.818 |
| Data reduction software | PROTEUM PLUS |
| Data scaling software | PROTEUM PLUS |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 17.730 | 1.830 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.042 | 0.489 |
| Number of reflections | 61204 | 9365 |
| <I/σ(I)> | 15.7 | |
| Completeness [%] | 99.6 | |
| Redundancy | 4.6 | |
| CC(1/2) | 0.998 | 0.571 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289 | 20% PEG6000, 1 M lithium chloride, 0.1 M MES, pH 6.0 |
