6NZS
Dextranase AoDex KQ11
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 298 |
Detector technology | PIXEL |
Collection date | 2017-04-06 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9789 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 214.071, 55.099, 62.188 |
Unit cell angles | 90.00, 92.45, 90.00 |
Refinement procedure
Resolution | 43.596 - 1.400 |
R-factor | 0.1683 |
Rwork | 0.168 |
R-free | 0.18250 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3wwg |
RMSD bond length | 0.005 |
RMSD bond angle | 0.824 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.11.1_2575) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.410 |
High resolution limit [Å] | 1.390 | 1.390 |
Rmerge | 0.052 | 0.420 |
Number of reflections | 143197 | |
<I/σ(I)> | 15.4 | |
Completeness [%] | 98.5 | |
Redundancy | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | magnesium chloride, HEPES, PEG |