6NZ4

YcjX-GDP (type I)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 19-ID
Synchrotron site	APS
Beamline	19-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-03-08
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9794
Spacegroup name	P 21 21 21
Unit cell lengths	59.314, 133.942, 144.620
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.859 - 1.920
R-factor	0.1812
Rwork	0.180
R-free	0.22280
RMSD bond length	0.004
RMSD bond angle	0.664
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.950
High resolution limit [Å]	1.920	1.920
Number of reflections	88457
<I/σ(I)>	28.3
Completeness [%]	99.3
Redundancy	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	287	50mM MES pH 6.0, 400mM Ammonium Chloride, 15% MEPEG 2K