6NTB
PII-like SbtB from Cyanobium sp PCC 7001 bound to ATP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-06-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 62 |
Unit cell lengths | 132.946, 132.946, 33.837 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 43.520 - 1.900 |
Rwork | 0.195 |
R-free | 0.22700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6mm2 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.520 | 1.940 |
High resolution limit [Å] | 1.900 | 1.900 |
Rmerge | 0.107 | |
Rmeas | 0.112 | |
Rpim | 0.035 | 0.925 |
Number of reflections | 27468 | 2714 |
<I/σ(I)> | 15.8 | 1.2 |
Completeness [%] | 100.0 | 100 |
Redundancy | 20 | 18.1 |
CC(1/2) | 0.999 | 0.560 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 0.2 M Lithium Chloride, 20 % PEG 6000, 100 mM sodium acetate-acetic acid, pH 5 |