6NFR
CopC from Pseudomonas fluorescens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2015-04-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9537 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 30.034, 35.565, 95.649 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.360 - 1.000 |
R-factor | 0.14995 |
Rwork | 0.149 |
R-free | 0.17178 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2c9q |
RMSD bond length | 0.006 |
RMSD bond angle | 1.240 |
Data reduction software | HKL-2000 (5.8.0230) |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | REFMAC |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.360 | 1.030 |
High resolution limit [Å] | 1.000 | 1.000 |
Number of reflections | 56023 | |
<I/σ(I)> | 12.2 | |
Completeness [%] | 92.7 | |
Redundancy | 2.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.7 | 293 | 2.5 M ammonium sulfate, 0.1 M Bis-Tris propane, pH 6.7 |