6MVN

LasR LBD L130F:3OC10HSL complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RUH3R
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2017-12-19
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.0
Spacegroup name	P 1 21 1
Unit cell lengths	42.664, 62.124, 51.315
Unit cell angles	90.00, 90.21, 90.00

Refinement procedure

Resolution	28.968 - 2.200
R-factor	0.1794
Rwork	0.176
R-free	0.23440
RMSD bond length	0.007
RMSD bond angle	1.024
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.9_1692)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.200
High resolution limit [Å]	2.200	2.130
Number of reflections	13464
<I/σ(I)>	17.4
Completeness [%]	96.4
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	200 mM magnesium nitrate, 20% PEG3350