6MQA

Structure of HIV-1 CA P207S

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-11-16
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	0.979200
Spacegroup name	P 6
Unit cell lengths	90.237, 90.237, 57.534
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	46.332 - 3.199
R-factor	0.1876
Rwork	0.186
R-free	0.21870
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4xfx
RMSD bond length	0.005
RMSD bond angle	1.049
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.12_2829: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	3.390
High resolution limit [Å]	3.199	3.199
Number of reflections	4519
<I/σ(I)>	6.61
Completeness [%]	98.9
Redundancy	2.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	15% PEG3350, 0.1 M sodium iodide, 0.1 M Bis-Tris propane