6M9I
L-GSTSTA from degenerate octameric repeats in InaZ, residues 707-712
Experimental procedure
| Collection date | 2017-09-24 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 9.190, 11.890, 22.430 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 0.900 - 0.900 |
| R-factor | 0.2188 |
| Rwork | 0.217 |
| R-free | 0.23240 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.057 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | SHELXD |
| Refinement software | PHENIX (1.12_2829) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 7.271 | 7.271 | 1.000 |
| High resolution limit [Å] | 0.900 | 5.000 | 0.900 |
| Rmerge | 0.162 | 0.106 | 0.357 |
| Rmeas | 0.185 | 0.126 | 0.409 |
| Total number of observations | 7513 | ||
| Number of reflections | 1760 | 9 | 452 |
| <I/σ(I)> | 5.5 | 9.03 | 3.09 |
| Completeness [%] | 85.5 | 45 | 83.7 |
| Redundancy | 4.269 | 3.111 | 4.206 |
| CC(1/2) | 0.990 | 0.997 | 0.726 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
