6M4J
SspA in complex with cysteine
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2016-04-01 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.9789 |
Spacegroup name | P 63 2 2 |
Unit cell lengths | 132.264, 132.264, 152.636 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 114.540 - 1.800 |
R-factor | 0.167 |
Rwork | 0.166 |
R-free | 0.19020 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3vax |
RMSD bond length | 0.012 |
RMSD bond angle | 1.765 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | REFMAC (5.6.0117) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 115.000 | 1.840 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 72776 | 11922 |
<I/σ(I)> | 5.3 | |
Completeness [%] | 100.0 | |
Redundancy | 12.5 | |
CC(1/2) | 0.962 | 0.962 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 287.15 | 1.8M ammonium citrate, pH 7.0 |