6LNL

ASFV core shell protein p15

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2019-10-23
Detector	Nonius Kappa CCD
Wavelength(s)	0.9792
Spacegroup name	C 1 2 1
Unit cell lengths	127.808, 57.017, 72.456
Unit cell angles	90.00, 116.18, 90.00

Refinement procedure

Resolution	19.758 - 1.929
R-factor	0.1901
Rwork	0.188
R-free	0.21910
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1xyz
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.760	1.970
High resolution limit [Å]	1.928	1.930
Rmerge	0.081
Number of reflections	34865	3121
<I/σ(I)>	14
Completeness [%]	98.4
Redundancy	6.6
CC(1/2)		0.996

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		293	0.1 M HEPES:NaOH pH 7.5 25% (w/v) PEG 3350