6LJQ

human galectin-16 R55N

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-10-31
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.98
Spacegroup name	C 1 2 1
Unit cell lengths	55.817, 34.333, 67.892
Unit cell angles	90.00, 102.06, 90.00

Refinement procedure

Resolution	19.270 - 1.490
R-factor	0.1787
Rwork	0.176
R-free	0.20830
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6ljp
Refinement software	PHENIX (1.17_3644)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.270	1.520
High resolution limit [Å]	1.490	1.490
Rmerge	0.076	0.461
Number of reflections	20576	978
<I/σ(I)>	8.4
Completeness [%]	99.3
Redundancy	3.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG