6LJG

Crassostrea gigas ferritin mutant-D119G

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	93
Detector technology	PIXEL
Collection date	2019-11-09
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9785
Spacegroup name	I 4 3 2
Unit cell lengths	151.134, 151.134, 151.134
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	26.717 - 1.799
R-factor	0.1936
Rwork	0.192
R-free	0.21470
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1fha
Data reduction software	HKL-3000
Data scaling software	HKL-3000
Phasing software	HKL-3000
Refinement software	PHENIX (1.14_3260)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	26.720	1.864
High resolution limit [Å]	1.799	1.799
Number of reflections	27659	2700
<I/σ(I)>	311
Completeness [%]	99.9
Redundancy	38.8
CC(1/2)	1.000	1.000

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	PEG 8000, CAPS/Sodium hydroxide, Sodium chloride