6LIJ
Crassostrea gigas ferritin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 93 |
| Detector technology | PIXEL |
| Collection date | 2018-12-21 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9785 |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 183.007, 183.007, 183.007 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 35.220 - 2.100 |
| R-factor | 0.1946 |
| Rwork | 0.193 |
| R-free | 0.23040 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1fha |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.724 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX (1.10.1_2155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 35.220 | 2.175 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 15887 | 1533 |
| <I/σ(I)> | 1.36 | |
| Completeness [%] | 100.0 | |
| Redundancy | 3 | |
| CC(1/2) | 0.750 | 0.750 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | Magnesium chloride hexahydrate, Tris(hydroxymethyl)aminomethane, 1,6-Hexanediol |
