6LHN

RLGSGG-AtPRT6 UBR box

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 5C (4A)
Synchrotron site	PAL/PLS
Beamline	5C (4A)
Temperature [K]	193
Detector technology	PIXEL
Collection date	2019-11-24
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.0
Spacegroup name	P 43 3 2
Unit cell lengths	95.414, 95.414, 95.414
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.950 - 2.500
R-factor	0.2164
Rwork	0.213
R-free	0.25030
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6KGG
RMSD bond length	0.012
RMSD bond angle	1.242
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHENIX
Refinement software	PHENIX ((1.14_3260: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.670	2.589
High resolution limit [Å]	2.499	2.500
Number of reflections	5522	5513
<I/σ(I)>	16.6
Completeness [%]	99.5
Redundancy	9
CC(1/2)	0.986	0.714

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	1.6M ammonium sulfate, 0.1M MES pH6.5