6LFN

Crystal structure of LpCGTb

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-14
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97851
Spacegroup name	P 2 21 21
Unit cell lengths	78.343, 87.821, 134.413
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.603 - 2.395
R-factor	0.2131
Rwork	0.211
R-free	0.25610
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6lf6
Data reduction software	DENZO
Data scaling software	HKL-3000
Phasing software	PHASER
Refinement software	PHENIX (1.13_2998)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.603	2.440
High resolution limit [Å]	2.395	2.395
Rpim	0.052	0.376
Number of reflections	36830	3211
<I/σ(I)>	14.8
Completeness [%]	99.0
Redundancy	6.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	0.2M Lithium sulfate monohydrate, 0.1M Tris pH 8.5, 25% w/v Polyethylene glycol 3350