6L55

Recombinant Tegillarca granosa ferritin

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	CCD
Collection date	2018-12-26
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.97890
Spacegroup name	C 2 2 2
Unit cell lengths	214.623, 214.905, 151.902
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.042 - 1.783
R-factor	0.205079920377
Rwork	0.204
R-free	0.23093
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1bg7
RMSD bond length	0.005
RMSD bond angle	0.781
Data reduction software	xia2
Data scaling software	HKL-3000
Phasing software	BALBES
Refinement software	PHENIX (1.10.1_2155)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.810
High resolution limit [Å]	1.780	1.780
Rmerge	0.092	0.158
Number of reflections	330028	13365
<I/σ(I)>	3.4	2
Completeness [%]	98.9	80.5
Redundancy	6.7	6.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289	4.0M Sodium formate