6KXB

Galectin-3 CRD binds to GalA trimer

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-06-19
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97
Spacegroup name	P 21 21 21
Unit cell lengths	35.880, 57.858, 61.562
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.340 - 1.500
R-factor	0.167
Rwork	0.165
R-free	0.20300
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	4r9a
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.340	1.530
High resolution limit [Å]	1.500	1.500
Rmerge	0.070	0.195
Number of reflections	21105
<I/σ(I)>	15.4
Completeness [%]	99.7
Redundancy	5.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	PEG