6KTB

Crystal structure of B. halodurans MntR in apo form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-12
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97960
Spacegroup name	P 21 21 21
Unit cell lengths	39.528, 89.370, 109.945
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	37.197 - 2.500
Rwork	0.171
R-free	0.21800
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.540
High resolution limit [Å]	2.500	2.500
Rmerge	0.128	0.367
Number of reflections	14131
<I/σ(I)>	14.1	7.9
Completeness [%]	99.9
Redundancy	6.6	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		296	sodium phosphate, magensium formate