6KTA

Crystal structure of B. halodurans MntR in apo form

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 11C
Synchrotron site	PAL/PLS
Beamline	11C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-12
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97941
Spacegroup name	P 21 21 21
Unit cell lengths	39.659, 89.203, 109.757
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	46.741 - 2.300
Rwork	0.189
R-free	0.22900
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.340
High resolution limit [Å]	2.300	2.300
Rmerge	0.119	0.364
Number of reflections	17942	115264
<I/σ(I)>	16.2	4.5
Completeness [%]	99.1
Redundancy	6.4	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		296	sodium/potassium phosphate, Magnesium formate