6KKG
Crystal structure of MAGI2-Dendrin complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-12-24 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91877 |
Spacegroup name | P 32 |
Unit cell lengths | 55.715, 55.715, 74.696 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.190 |
High resolution limit [Å] | 2.150 | 5.830 | 2.150 |
Rmerge | 0.082 | 0.071 | 0.455 |
Rmeas | 0.095 | 0.082 | 0.528 |
Rpim | 0.047 | 0.039 | 0.265 |
Number of reflections | 13900 | 705 | 684 |
<I/σ(I)> | 7.2 | ||
Completeness [%] | 98.6 | 99.2 | 100 |
Redundancy | 4.2 | 4.2 | 4 |
CC(1/2) | 0.988 | 0.856 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289 | 2.2M Ammonium Sulfate, 150mM Malate at pH 5.1, 4.0% v/v 1,2-Propanedio |