6KJW

Galectin-13 variant C136S

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-21
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97
Spacegroup name	P 43 21 2
Unit cell lengths	53.438, 53.438, 113.839
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.501 - 1.360
R-factor	0.1939
Rwork	0.193
R-free	0.20170
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.047
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	19.501	1.380
High resolution limit [Å]	1.360	1.360
Number of reflections	36278	1753
<I/σ(I)>	28.8
Completeness [%]	99.9
Redundancy	6.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		298	Bis-Tris