6KD1
Room temperature structure of lysozyme delivered in agarose by serial millisecond crystallography
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 298.15 |
Detector technology | PIXEL |
Collection date | 2019-04-03 |
Detector | DECTRIS PILATUS3 X 6M |
Wavelength(s) | 0.9796 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.740, 79.740, 38.560 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.385 - 1.850 |
R-factor | 0.1762 |
Rwork | 0.173 |
R-free | 0.22440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6ig6 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.600 | 1.910 |
High resolution limit [Å] | 1.850 | 1.850 |
Number of reflections | 11117 | 1068 |
<I/σ(I)> | 6.33 | |
Completeness [%] | 100.0 | 100 |
Redundancy | 361.4 | 250.4 |
CC(1/2) | 0.995 | 0.823 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 293.5 | sodium acetate, PEG 8000, NaCl |