6KAW
Crystal structure of CghA
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-17A |
| Synchrotron site | Photon Factory |
| Beamline | BL-17A |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2016-12-14 |
| Detector | DECTRIS PILATUS3 S 6M |
| Wavelength(s) | 0.98000 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 76.016, 76.016, 190.282 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 20.000 - 2.010 |
| R-factor | 0.1916 |
| Rwork | 0.190 |
| R-free | 0.21840 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.067 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.130 |
| High resolution limit [Å] | 2.010 | 2.010 |
| Rmerge | 0.181 | 0.864 |
| Number of reflections | 38207 | 5995 |
| <I/σ(I)> | 10.4 | |
| Completeness [%] | 99.8 | |
| Redundancy | 13 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 4000, MES |
