6K11
Crystal structure of MvcA from Legionella pneumophila
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL17U |
| Synchrotron site | SSRF |
| Beamline | BL17U |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-12-05 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97894 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 122.652, 135.230, 66.903 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 58.733 - 1.936 |
| R-factor | 0.2039 |
| Rwork | 0.202 |
| R-free | 0.23810 |
| Structure solution method | SAD |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.798 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | SHELXS |
| Refinement software | PHENIX ((1.11.1_2575: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.733 | 2.040 |
| High resolution limit [Å] | 1.936 | 1.940 |
| Number of reflections | 83566 | 12059 |
| <I/σ(I)> | 14.4 | |
| Completeness [%] | 99.9 | |
| Redundancy | 13.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | COUNTER-DIFFUSION | 289.15 | 30%(v/v)Jeffamine M-600 PH7.0 100mM HEPES/Sodium hydroxide PH7.0 |
