6K09

Crystal structure B of ceNAP1-H2A-H2B complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-15
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9790
Spacegroup name	P 21 21 21
Unit cell lengths	68.795, 79.180, 172.340
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.723 - 2.248
R-factor	0.2157
Rwork	0.214
R-free	0.24850
Structure solution method	MOLECULAR REPLACEMENT
Data reduction software	HKL-2000
Data scaling software	SCALA
Phasing software	PHASER
Refinement software	PHENIX (1.14_3260: ???)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.723	2.330
High resolution limit [Å]	2.248	2.248
Rmerge		0.557
Number of reflections	45336	45336
<I/σ(I)>	25.14
Completeness [%]	99.4
Redundancy	11

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	20% PEG 3350