6JQS

Structure of Transcription factor, GerE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	200
Detector technology	CCD
Collection date	2015-10-14
Detector	ADSC QUANTUM 270
Wavelength(s)	0.97934
Spacegroup name	P 64
Unit cell lengths	63.769, 63.769, 45.407
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	21.000 - 2.090
R-factor	0.20562
Rwork	0.203
R-free	0.25069
RMSD bond length	0.012
RMSD bond angle	1.808
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Refinement software	REFMAC (5.8.0238)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.000	2.040
High resolution limit [Å]	2.010	2.010
<I/σ(I)>	35.3
Completeness [%]	99.6
Redundancy	7.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	0.18 M sodium chloride and 18% (w/v) PEG 3350