6JQ8
Crystal structure of HddC from Yersinia pseudotuberculosis complexed with GMP-PN
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-05-03 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 0.97928 |
Spacegroup name | P 43 |
Unit cell lengths | 80.526, 80.526, 53.081 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.319 - 1.546 |
R-factor | 0.2076 |
Rwork | 0.207 |
R-free | 0.22880 |
RMSD bond length | 0.006 |
RMSD bond angle | 0.899 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.320 | |
High resolution limit [Å] | 1.546 | 1.546 |
Number of reflections | 49164 | |
<I/σ(I)> | 43.89 | |
Completeness [%] | 96.2 | |
Redundancy | 12.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 296 | 0.05M HEPES pH 7.5, 0.05M MgCl2, 1.2M Sodium Citrate |