6JJN

Crystal structure of Mumps virus hemagglutinin-neuraminidase bound to sialyl lewisX

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B2
Synchrotron site	SPring-8
Beamline	BL26B2
Temperature [K]	100
Detector technology	CCD
Collection date	2017-07-15
Detector	RAYONIX MX225-HS
Wavelength(s)	1
Spacegroup name	P 61
Unit cell lengths	137.417, 137.417, 177.807
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	49.450 - 2.500
R-factor	0.1759
Rwork	0.174
R-free	0.20460
RMSD bond length	0.003
RMSD bond angle	0.681
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.540
High resolution limit [Å]	2.500	2.500
Number of reflections	65599
<I/σ(I)>	19
Completeness [%]	100.0
Redundancy	20.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		293	sodium acetate, ammonium sulfate, glycerol