6JJ6

BRD4 in complex with 500

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-26
Detector	DECTRIS PILATUS3 S 6M
Wavelength(s)	0.9793
Spacegroup name	P 21 21 21
Unit cell lengths	31.800, 47.120, 79.190
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.494 - 1.400
R-factor	0.183
Rwork	0.182
R-free	0.20130
Data reduction software	TRUNCATE
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX (1.14_3235)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.494	1.450
High resolution limit [Å]	1.400	1.400
Number of reflections	24087
<I/σ(I)>	8.12
Completeness [%]	99.7
Redundancy	2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	4.0M HCOONa