6JG5

Crystal structure of AimR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-10-28
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9792
Spacegroup name	P 21 21 2
Unit cell lengths	115.302, 219.429, 33.494
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.537 - 2.221
R-factor	0.1983
Rwork	0.196
R-free	0.23940
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	5xyb
RMSD bond length	0.009
RMSD bond angle	0.956
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.14rc3_3206: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.290
High resolution limit [Å]	2.220	2.220
Number of reflections	42901
<I/σ(I)>	10.9
Completeness [%]	99.1
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		291.15	Sodium cacodylate, PEG 8000, sodium chloride