6J9K
Apo-AcrIIC2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL18U1 |
| Synchrotron site | SSRF |
| Beamline | BL18U1 |
| Temperature [K] | 193 |
| Detector technology | PIXEL |
| Collection date | 2017-08-22 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9785 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 72.022, 72.022, 105.230 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.217 - 2.234 |
| R-factor | 0.2095 |
| Rwork | 0.206 |
| R-free | 0.24290 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.213 |
| Data scaling software | HKL-3000 |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.8.1_1168) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.300 |
| High resolution limit [Å] | 2.230 | 2.230 |
| Rmerge | 0.094 | 4.078 |
| Number of reflections | 8250 | 599 |
| <I/σ(I)> | 28.9 | |
| Completeness [%] | 98.3 | 81.3 |
| Redundancy | 35.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Tris, ethanol |
