6J9K

Apo-AcrIIC2

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL18U1
Synchrotron site	SSRF
Beamline	BL18U1
Temperature [K]	193
Detector technology	PIXEL
Collection date	2017-08-22
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.9785
Spacegroup name	P 63 2 2
Unit cell lengths	72.022, 72.022, 105.230
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	40.217 - 2.234
R-factor	0.2095
Rwork	0.206
R-free	0.24290
Structure solution method	SAD
RMSD bond length	0.010
RMSD bond angle	1.213
Data scaling software	HKL-3000
Phasing software	PHENIX
Refinement software	PHENIX (1.8.1_1168)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.300
High resolution limit [Å]	2.230	2.230
Rmerge	0.094	4.078
Number of reflections	8250	599
<I/σ(I)>	28.9
Completeness [%]	98.3	81.3
Redundancy	35.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.1M Tris, ethanol