Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE BL-5A |
| Synchrotron site | Photon Factory |
| Beamline | BL-5A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-11-29 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 33.039, 54.446, 66.070 |
| Unit cell angles | 90.00, 100.39, 90.00 |
Refinement procedure
| Resolution | 20.000 - 1.201 |
| R-factor | 0.1343 |
| Rwork | 0.133 |
| R-free | 0.15680 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 2g8c |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.931 |
| Data scaling software | HKL-2000 |
| Refinement software | PHENIX ((1.12_2829: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.220 |
| High resolution limit [Å] | 1.200 | 1.200 |
| Rmerge | 0.047 | 0.156 |
| Number of reflections | 70798 | 3461 |
| <I/σ(I)> | 28.2 | 11.6 |
| Completeness [%] | 98.5 | 96.5 |
| Redundancy | 3.7 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 38% PEG 400, 0.1 M Tris pH 8.0 |
