6J1V

The structure of HLA-A*3003/RT313

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2018-01-10
Detector	SDMS
Wavelength(s)	0.97853
Spacegroup name	P 21 21 21
Unit cell lengths	52.263, 72.129, 124.679
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	48.200 - 2.000
R-factor	0.2021
Rwork	0.201
R-free	0.21700
RMSD bond length	0.007
RMSD bond angle	0.803
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	CNS
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.070
High resolution limit [Å]	2.000	2.000
Number of reflections	32751
<I/σ(I)>	0.2
Completeness [%]	99.8
Redundancy	7.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7.5	291	0.1 M HEPES (pH 7.5), 25% (w/v) polyethylene glycol 3350