6IZE

Dimeric human TCTP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PAL/PLS BEAMLINE 7A (6B, 6C1)
Synchrotron site	PAL/PLS
Beamline	7A (6B, 6C1)
Temperature [K]	100
Detector technology	CCD
Collection date	2013-04-04
Detector	MARMOSAIC 325 mm CCD
Wavelength(s)	0.97933
Spacegroup name	P 43
Unit cell lengths	55.772, 55.772, 195.820
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	32.051 - 2.290
R-factor	0.2187
Rwork	0.215
R-free	0.27310
RMSD bond length	0.012
RMSD bond angle	1.317
Data reduction software	MOSFLM
Data scaling software	pointless
Phasing software	PHENIX
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	55.720	2.370
High resolution limit [Å]	2.290	2.290
Number of reflections	29992
<I/σ(I)>	25.6
Completeness [%]	99.9
Redundancy	13.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	296	0.1 M MES pH 6.5, 0.2 M ammonium acetate, 25 % (w/v) PEG 1500