6IZB

Flexible loop truncated human TCTP

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	SwissFEL ARAMIS BEAMLINE ESA
Synchrotron site	SwissFEL ARAMIS
Beamline	ESA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2011-05-21
Detector	DECTRIS PILATUS3 R CdTe 300K
Wavelength(s)	1.000
Spacegroup name	P 61 2 2
Unit cell lengths	69.295, 69.295, 146.062
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	46.366 - 1.899
R-factor	0.2209
Rwork	0.220
R-free	0.24590
RMSD bond length	0.019
RMSD bond angle	1.187
Data reduction software	iMOSFLM
Data scaling software	pointless
Phasing software	PHENIX
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	46.370	1.970
High resolution limit [Å]	1.900	1.900
Number of reflections	17029
<I/σ(I)>	45.7
Completeness [%]	99.5
Redundancy	36.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	296	0.1 M MES pH 6.5, 25 % (w/v) PEG 300