6IPQ
Non-native ferritin 8-mer mutant-C90A/C102A/C130A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 77 |
| Detector technology | PIXEL |
| Collection date | 2018-06-17 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.9779 |
| Spacegroup name | F 4 3 2 |
| Unit cell lengths | 181.844, 181.844, 181.844 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 40.600 - 3.103 |
| R-factor | 0.2003 |
| Rwork | 0.196 |
| R-free | 0.27580 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.236 |
| Data reduction software | HKL-3000 |
| Data scaling software | HKL-3000 |
| Phasing software | HKL-3000 |
| Refinement software | PHENIX ((1.10.1_2155: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.600 | 3.200 |
| High resolution limit [Å] | 3.100 | 3.100 |
| Number of reflections | 5057 | |
| <I/σ(I)> | 4.7 | |
| Completeness [%] | 99.0 | |
| Redundancy | 20.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 293 | 200mM MgCl2, 3.4M 1,6-Hexanediol, 100mM Tris/HCl |
