6IDX
Crystal Structure of BAI1/ELMO2 complex
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NFPSS BEAMLINE BL18U |
| Synchrotron site | NFPSS |
| Beamline | BL18U |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-11-04 |
| Detector | DECTRIS PILATUS3 X 1M |
| Wavelength(s) | 0.97853 |
| Spacegroup name | P 31 2 1 |
| Unit cell lengths | 92.869, 92.869, 130.762 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 46.435 - 1.699 |
| R-factor | 0.1806 |
| Rwork | 0.179 |
| R-free | 0.20640 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 6ie1 |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.157 |
| Data reduction software | d*TREK |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.8.4_1496) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.435 | 1.730 |
| High resolution limit [Å] | 1.699 | 1.699 |
| Rmerge | 0.068 | 0.640 |
| Number of reflections | 72368 | 3592 |
| <I/σ(I)> | 28.4 | |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 9.9 | 10 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.3M Ammonium Fluoride, 18% PEG3,350 |
