6I0T

Crystal structure of DmTailor in complex with GpU

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-02-26
Detector	DECTRIS PILATUS 2M-F
Wavelength(s)	1.00003
Spacegroup name	P 31 2 1
Unit cell lengths	60.425, 60.425, 162.284
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	43.977 - 2.000
R-factor	0.2057
Rwork	0.204
R-free	0.23310
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	6i0s
RMSD bond length	0.007
RMSD bond angle	0.865
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.14_3211: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.000	2.070
High resolution limit [Å]	2.000	2.000
Number of reflections	24045
<I/σ(I)>	18.48	1.17
Completeness [%]	100.0	100
Redundancy	16.5	16.5
CC(1/2)	1.000	0.392

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	7	293	30% (v/v) glycerol ethoxylate, 60 mM sodium malonate, pH7.0