6HP5

ARBITRIUM PEPTIDE RECEPTOR FROM SPBETA PHAGE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2017-12-12
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.97925
Spacegroup name	P 41 21 2
Unit cell lengths	94.340, 94.340, 249.950
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	88.260 - 2.280
R-factor	0.19222
Rwork	0.190
R-free	0.22577
Structure solution method	SAD
RMSD bond length	0.014
RMSD bond angle	1.673
Data reduction software	XDS
Data scaling software	SCALA
Phasing software	CRANK2
Refinement software	REFMAC (5.8.0158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	88.262	2.320
High resolution limit [Å]	2.280	2.280
Number of reflections	52488
<I/σ(I)>	14.8
Completeness [%]	100.0
Redundancy	17.9

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		294	peg 3500, ammonium sulfate