6HNQ
TarP-6RboP-(CH2)6NH2
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-01-30 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 1.00002 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 95.410, 211.250, 122.680 |
| Unit cell angles | 90.00, 91.61, 90.00 |
Refinement procedure
| Resolution | 48.510 - 2.400 |
| R-factor | 0.18593 |
| Rwork | 0.184 |
| R-free | 0.22781 |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.314 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.500 | 2.460 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Number of reflections | 188717 | |
| <I/σ(I)> | 10.84 | |
| Completeness [%] | 99.9 | |
| Redundancy | 6.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 25% PEG 3350, 250 mM magnesium chloride, 0.1 M sodium citrate, pH 5.7 |
