6HEE

Crystal structure of Extracellular Domain 1 (ECD1) of FtsX from S. pneumonie in complex with undecyl-maltoside

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ALBA BEAMLINE XALOC
Synchrotron site	ALBA
Beamline	XALOC
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-09-13
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97934
Spacegroup name	P 43 21 2
Unit cell lengths	84.610, 84.610, 106.189
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	42.310 - 2.300
R-factor	0.2626
Rwork	0.261
R-free	0.29760
Starting model (for MR)	6he6
RMSD bond length	0.008
RMSD bond angle	0.987
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.13_2998: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	42.310	2.380
High resolution limit [Å]	2.300	2.300
Rpim	0.004	0.092
Number of reflections	17731
<I/σ(I)>	44.14
Completeness [%]	98.9
Redundancy	22.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291.15	ammonium sulfate, sodium and potassium tartrate and sodium citrate