6H9W
Unraveling the role of the secretor antigen in human rotavirus attachment to histo-blood group antigens
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97923 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 76.148, 76.148, 70.084 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 65.950 - 1.350 |
R-factor | 0.2069 |
Rwork | 0.206 |
R-free | 0.22730 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2i2s |
RMSD bond length | 0.032 |
RMSD bond angle | 2.703 |
Data reduction software | XDS |
Data scaling software | Aimless (5.8.0158) |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 65.950 | 1.420 |
High resolution limit [Å] | 1.350 | 1.350 |
Rpim | 0.021 | 0.266 |
Number of reflections | 52302 | 7527 |
<I/σ(I)> | 15.9 | 1.9 |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 10 | 5.8 |
CC(1/2) | 0.999 | 0.932 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294.15 | 1.2M (NH 4 ) 2 SO 4 3% iso-propanol and 0.1M sodium citrate pH4.6 |