6H89
MamM CTD D249N - Copper form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-02-01 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.975 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 36.732, 94.631, 53.521 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.320 - 1.700 |
R-factor | 0.19816 |
Rwork | 0.196 |
R-free | 0.24582 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3w5x |
RMSD bond length | 0.015 |
RMSD bond angle | 1.609 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0216) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.320 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.040 | |
Number of reflections | 10686 | |
<I/σ(I)> | 20.9 | 1.4 |
Completeness [%] | 99.7 | 95 |
Redundancy | 6.4 | 5.8 |
CC(1/2) | 0.999 | 0.753 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M AmSu, 0.1M BIS-TRIS pH=5.5, 25% PEG 3350, 1.7mM CuSO4 |